光子学报, 2019, 48 (10): 1005001, 网络出版: 2019-11-14  

基于铋纳米颗粒的自由沉降法制作X射线吸收光栅

Fabrication of X-ray Absorption Gratings by Free Settling of Bismuth Nanoparticles
作者单位
深圳大学 物理与光电工程学院 光电子器件与系统(教育部/广东省)重点实验室,广东 深圳 518060
摘要
利用深反应离子刻蚀技术或湿法腐蚀在硅上制作光栅结构,将与光栅浸润的液体作为载体携带铋纳米颗粒进入光栅结构内,形成致密排列,从而制作出X射线吸收光栅.致密地填充了周期为42 μm、刻蚀深度为150 μm的光栅结构,比较了其与微铸造法制作的铋块体吸收光栅的X射线吸收性能,并通过填充周期为24 μm和6 μm的光栅结构,研究了光栅周期与填充致密性之间的关系.扫描电镜测试结果显示自由沉降法可有效制作较大周期光栅,但对周期为6 μm光栅结构填充的致密性不佳。分析结果表明,对于小周期吸收光栅,需筛选所用填充颗粒,以保证颗粒粒径远小于光栅槽宽.基于纳米颗粒的自由沉降法可降低光栅制作成本及技术门槛,方便实现大面积吸收光栅的制作.
Abstract
To fabricate X-ray absorption gratings, deep reactive ion etching and wet etching are used to fabricate grating structures on silicon wafers, and a liquid carrier, which is wet with the surface of grating structure, is used to bring the bismuth nanoparticles into grating structures in a dense arrangement. Then, a grating structure with the period of 42 μm and depth of 150 μm is filled. To show the performance of the fabricated absorption grating, a comparison with the bulk bismuth grating obtained by micro-casting method is provided. Moreover, the relationship between the grating period and the filling compactness through filling grating structures with periods of 24 μm and 6 μm is found. The scanning electron microscopy micrographs show the effectiveness of free settling method for the large-period grating structures. However, for the structures with 6 μm period, the filling compactness is not satisfied. The results illustrate that bismuth nanoparticles that their diameters are much less than the width of grating structures should be selected for the small-period absorption gratings. Furthermore, nanoparticles-based free settling method lowers grating cost and technique threshold, and allows the fabrication of large-area absorption gratings.

雷耀虎, 许桂雯, 李乔飞, . 基于铋纳米颗粒的自由沉降法制作X射线吸收光栅[J]. 光子学报, 2019, 48(10): 1005001. 雷耀虎, 许桂雯, 李乔飞, WALI Faiz. Fabrication of X-ray Absorption Gratings by Free Settling of Bismuth Nanoparticles[J]. ACTA PHOTONICA SINICA, 2019, 48(10): 1005001.

关于本站 Cookie 的使用提示

中国光学期刊网使用基于 cookie 的技术来更好地为您提供各项服务,点击此处了解我们的隐私策略。 如您需继续使用本网站,请您授权我们使用本地 cookie 来保存部分信息。
全站搜索
您最值得信赖的光电行业旗舰网络服务平台!