光子学报, 2018, 47 (8): 0847013, 网络出版: 2018-09-16   

半球空腔约束对激光诱导玻璃等离子体辐射增强特性的研究

Effects of Hemispherical Confinement on the Enhancement of Laser-induced Glass Plasma Radiation
作者单位
河南科技大学 物理工程学院, 河南 洛阳 471023
摘要
为了增强激光诱导玻璃等离子体的辐射光谱信号, 采用直径为10 mm的玻璃纤维材质半球空腔对等离子体进行束缚, 对比研究了无约束和约束两种实验条件下的辐射光谱信号.由于激光的聚焦情况对玻璃等离子体特性有较大影响, 实验首先对激光在样品中的聚焦位置进行了优化, 结果表明当样品表面位于透镜焦平面以上3 mm处时激光诱导玻璃等离子体辐射光谱最强.然后采用时间分辨光谱对比研究了无约束和半球空腔约束下光谱强度的时间演变规律, 并分析了谱线强度增大倍数的时间演变, 结果表明在等离子体产生后6~15 μs的时间内, 半球空腔约束下谱线强度呈现出增强的现象, 且具有不同能级的谱线增强程度不同, 当采集延时为10 μs时具有最优增强效果.最后研究了激光能量对半球空腔约束下等离子体辐射增强效果的影响, 研究结果表明, 随着激光能量增大, 谱线增强倍数逐渐增加, 当激光能量超过170 mJ以后, 谱线增强效果开始下降.
Abstract
In order to enhance the radiation spectrum signal of laser-induced glass plasma, a hemispherical cavity which was made of glass fiber with a diameter of 10 mm was used to confine the plasma. The spectrum signals with confinement and without confinement were compared. Since the focusing of the laser has a great influence on the properties of the glass plasma, the focusing position of the laser in the sample was first optimized. The results show that when the sample surface is 3 mm above the focal plane of the lens, the spectral singnal from the laser-induced glass plasma was the strongest. Then the temporal evolution of spectral intensity under unconstrained and spatially constrained by a hemispherical cavity with the inner diameter of 10 mm was studied. The time evolution of the enhancement factor og the spectral intensity was analyzed. The results show that the spectral lines with confiment presents an enhanced phenomenon in the period of 6~15 μs after plasma generation. And the degree of enhancement of spectral lines with different energy levels is different. The maximum enhancement is achieved when the acquisition delay is 10 μs. Finally, the effect of laser energy on the enhancement of plasma radiation was studied. The results show that with the increase of laser energy, the enhancement factor of the spectral line is gradually increased. When the laser energy exceeds 170 mJ, the spectral enhancement effect begins to decrease.
参考文献

[1] HERVE K S, KRISHNA K A, FANG Y Y, et al. Analysis of slags using laser-induced breakdown spectroscopy[J]. Spectrochimica Acta Part B, 2016, 115(1): 40-45.

[2] ARAB M, BIDIN N, KASHIF C, et al. Characterization of pollution indices in soil surrounding a power plant by laser induced breakdown spectroscopy[J]. Analytical Letters, 2015 , 53 (2) : 360-370.

[3] RANULFI A C, ROMANO R A, BEBEACHIBULI M A,et al. Evaluation of the nutritional changes caused by Huanglongbing (HLB) to citrus plants using laser-induced breakdown spectroscopy[J]. Applied Spectroscopy, 2017 , 71 (7) : 1471-1480.

[4] MORIHISA S, AKIO I, CHIKARA I,et al. Development of a fiber-coupled laser-induced breakdown spectroscopy instrument for analysis of underwater debris in a nuclear reactor core[J]. Journal of Nuclear Science and Technology, 2014, 51 (7-8): 930-938.

[5] BASSEL L, MOTTO V, TRICHARD F, et al. Laser-induced breakdown spectroscopy for elemental characterization of calcitic alterations on cave walls[J]. Environmental Science and Pollution Research International, 2017, 24(3): 2197-2204.

[6] BRIDGE C M , POWELL J, STEELE K L, et al. Characterization of automobile float glass with laser-induced breakdown spectroscopy and laser ablation inductively coupled plasma mass spectrometry[J]. Applied Spectroscopy, 2006, 60 (10): 1181–1187.

[7] CARMONA N, OUJIA M, GASPARD S,et al. Lead determination in glasses by laser-induced breakdown spectroscopy[J]. Spectrochimica Acta Part B, 2007, 62(2): 94-100.

[8] JUNG E C, LEE D H, YUN J I,et al. Quantitative determination of uranium and europium in glass matrix by laser-induced breakdown spectroscopy[J]. Spectrochimica Acta Part B, 2011, 66(9): 761-764.

[9] CHOI I, CHAN G C, MAO X, et al. Line selection and parameter optimization for trace analysis of uranium in glass matrices by laser-induced breakdown spectroscopy(LIBS) [J]. Applied Spectroscopy, 2013, 67(11): 1275-1284.

[10] 李超, 王吉, 张炜,等. 激光诱导击穿光谱结合自由定标法同时定量分析玻璃主要元素[J]. 光子学报, 2016,45(4): 0414005.

    LI Chao, WANG Ji, ZHANG Wei, et al. Simultaneously quantitative analysis on the main elements in glass with Laser-induecd breakdown spectroscopy combined with calibration-free method [J]. Acta Photonica Sinica, 2016,45(4): 0414005.

[11] MATIASKE A M, GORNUSHKIN I B, PANNE U. Double-pulse laser-induced breakdown spectroscopy for analysis of molten glass[J].Analytical & Bioanalytical Chemistry, 2012, 402(8): 2597-2606.

[12] 李嘉铭, 褚应波, 赵楠, 等. 激光诱导荧光辅助激光诱导击穿光谱检测有源发光玻璃中的微量元素[J]. 分析化学, 2016, 44(7): 1042-1046.

    LI Jia-ming, CHU Ying-bo, ZHAO Nan,et al. Detection of trace elements in active luminescent glass using laser-induced breakdown spectroscopy combined with laser-induced fluorescence[J]. Chinese Journal of Analytical Chemistry, 2016, 44(7): 1042-1046.

[13] GAO X, LIU L, SONG C,et al. The role of spatial confinement on nanosecond YAG laser-induced Cu plasma[J]. Journal of Physics D: Applied Physics, 2015, 48(17): 175205.

[14] LI A, GUO S, WAZIR N,et al. Accuracy enhancement of laser induced breakdown spectra using permittivity and size optimized plasma confinement rings[J]. Optics Express, 2017, 25(22): 27559.

[15] WANG Z, HOU Z, LUI S,et al. Utilization of moderate cylindrical confinementfor precision improvement of laser-induced breakdown spectroscopy signal[J]. Optics Express, 2012, 20(s6): A1012.

[16] GUO L B, HAO Z Q, SHEN M,et al. Accuracy improvement of quantitative analysis by spatial confinement in laser-induced breakdown spectroscopy[J]. Optics Express, 2013, 21(15) : 018188.

[17] GUO L B, LI C M, HUW, et al. Plasma confinement by hemispherical cavity in laser-induced breakdown spectroscopy[J]. Applied Physics Letter, 2011, 98: 131501.

[18] ROSALIE A M, LEEANN E F, DAVID A C, et al. Effect of sampling geometry on elemental emissions in laser-induced breakdown spectroscopy[J]. Applied Spectroscopy, 1996, 50(12): 1483–1499.

[19] 刘月华, 陈明, 刘向东, 等.透镜到靶材的距离对脉冲激光诱导等离子体的影响机理研究[J].物理学报,2013,62(2): 025203.

    LIU Yue-hua, CHEN Ming, LIU Xiang-dong,et al. The mechanism of effect of lens-to-sample distance on laser-induced plasma[J]. Acta Physics Sinica, 2013,62(2): 025203.

[20] 王静鸽, 陈兴龙, 付洪波, 等. 透镜到样品的距离对激光诱导等离子体的影响[J]. 光学学报, 2014, 34(9): 0930006.

    WANG Jing-ge, CHEN Xing-long, FU Hong-bo, et al. Influence of the lens-to-sample distance on the laser-induecd plasma[J].Acta Optica Sinica, 2014, 34(9): 0930006.

[21] ABDELLATIF G, IMAM H. A study of the laser plasma parameters at different laser wavelengths[J].Spectrochimica Acta Part B, 2002, 57(7), 1155-1165.

王静鸽, 李小龙, 胡俊涛, 李新忠. 半球空腔约束对激光诱导玻璃等离子体辐射增强特性的研究[J]. 光子学报, 2018, 47(8): 0847013. WANG Jing-ge, LI Xiao-long, HU Jun-tao, LI Xin-zhong. Effects of Hemispherical Confinement on the Enhancement of Laser-induced Glass Plasma Radiation[J]. ACTA PHOTONICA SINICA, 2018, 47(8): 0847013.

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